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Table 1 shows the analytical parameters resulting from xilverster calibration graphs in Figure 1. The response in the absence of ammonia is shown as a dashed line. Interestingly the sloping steady state response on the MATFE was not observed for a conventional redox system e. The mixture was then passed through an additional gas-mixing segment [ 41 ] to increase turbulence and to ensure adequate mixing of both gases.
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To confirm the sensing behaviour silversrer ammonia, 1 mM of a standard redox probe, ferrocene was also studied in acetonitrile with 0. Sensitivities were calculated from the gradient of the line of best fit and limits of detection LODs were calculated from three times standard deviation of the intercept. The electrochemical cell was placed inside an aluminium Faraday cage in the fume cupboard to reduce electrical interference.